CH 223 |
Chemical Technology Lab - I |
0-0-6-6 |
Syllabus: Identification of unknown organic compounds: element detection,
confirmation of the functional groups, derivatization; Separation
technique: normal and reduced pressure distillation, solubility method,
column chromatography method, sublimation; Isolation of medicinal compounds
from plants/other sources: Soxhlet extraction; Preparation:
aspirin, paracetamol, imidazole, dye preparation; multistep
synthesis; Estimation of organic compounds: paracetamol, glucose;
Characterization of unknown organic compounds by UV-Vis, IR and 1H-NMR
techniques; Experiment based on polymer science, electrophoresis, protein
estimation, catalytic hydrogenation. Texts and References: 1. J. R. Mohrig, T. C. Morrill, C. N. Hammond and
D.C. Neckers, Experimental organic chemistry, W.H. Freeman
and Co. ,1998. 2. N. K. Vishnoi, Advanced practical organic chemistry, Vikash publishing
house Pvt. Ltd. ,1996. 3. B. S. Furniss, A.J. Hannaford, P.W.G. Smith, and
A.R. Tatchell, Vogel's textbooks of practical organic chemistry, 5th Ed., ELBS Longman ,1994. |